Tersus Assigned Patents & Trademarks
Tersus Environmental holds patents covering technologies and methods developed for in situ remediation of contaminated soil and groundwater. These patents address treatment approaches involving enhanced reductive bioremediation, zero-valent metals, thermal processes, and surfactant-enhanced remediation.
The listings below identify patents assigned to Tersus Environmental and trademarks associated with our remediation products and technologies.
Tersus Assigned Patents
Tersus Environmental’s patents reflect the development and application of proprietary technologies and methods for in situ remediation of soil and groundwater contamination. These patents document technical innovations derived from applied field experience, research, and product development activities.
The patents listed below represent key intellectual property associated with Tersus Environmental’s remediation technologies and treatment approaches.
Patent No. : US 12,753,344 B2 · Issued Oct 6, 2026
Method for Heat Enhanced Reductive Bioremediation
Gary M. Birk; David F. Alden; John Sankey; and Guilherme Mascalchi de Figueiredo
View Description
This patent describes a method for enhancing in situ reductive bioremediation through the injection of heated vegetable oil emulsions combined with alkaline-catalyzed reactions to promote contaminant degradation in soil and groundwater.
The technology involves heating a mixture of vegetable oil, emulsifier, and water aboveground before injection into the contaminated formation. The heated mixture raises subsurface temperatures and maintains elevated temperatures within the treatment zone without continuous external heating.
An alkaline catalyst containing an alcohol is introduced to promote in situ alcoholysis reactions that generate fatty acid alkyl esters, glycerol, and carboxylic acid salts. These reaction products provide readily available and longer-lasting electron donors to support anaerobic microbial activity and enhanced reductive dechlorination of chlorinated solvents.
The approach combines thermal enhancement, electron donor delivery, and in situ chemical reactions to improve substrate distribution, promote biological degradation, and potentially reduce remediation timeframes.
Patent No.: CA 3,109,644 · Issued Aug 18, 2026
Enhanced reduction bioremediation method using in-situ alcoholysis
Gary Birk and David Alden
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This Canadian patent describes a method for enhancing in situ reductive bioremediation through alcoholysis reactions that convert vegetable oils into a combination of soluble and slow-release electron donors within contaminated soil and groundwater.
The technology combines water-miscible vegetable oils, alcohols, and catalysts to promote the formation of fatty acid alkyl esters, glycerol, and carboxylic acid salts. These reaction products provide both readily available and longer-lasting electron donors to support anaerobic microbial processes, including enhanced reductive dechlorination of chlorinated solvents.
The approach is designed to improve electron donor distribution within the aquifer, sustain reducing conditions, and provide buffering capacity to help maintain groundwater pH favorable for microbial activity.
The technology provides an alternative to conventional emulsified vegetable oil (EVO) applications by combining electron donor delivery with in situ chemical reactions that support contaminant biodegradation.
Patent No.: US 12,522,766 B2 · Issued Jan 13, 2026
Method for Preparation of Oil-in-Water Emulsions for Promoting an Environment for Bioremediation of a Contamination
Gary M. Birk, David F. Alden, Luca Collin Condes, Michale Taylor Warren, and Jeffrey Harry Harwell
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This patent describes a method for preparing surfactant-free oil-in-water emulsions for enhanced in situ bioremediation of contaminated soil and groundwater.
The technology uses a controlled degassing process to remove dissolved gases from water and vegetable oil before mixing. This allows the formation of an oil-in-water emulsion without conventional surfactants or emulsifying agents.
The resulting emulsion is designed to improve the subsurface distribution of vegetable oil electron donors, promoting anaerobic conditions and stimulating microbial processes responsible for contaminant degradation, including enhanced reductive dechlorination of chlorinated solvents.
The approach offers an alternative to conventional emulsified vegetable oil (EVO) formulations by eliminating the need for added surfactants while providing a means of delivering electron donor substrates into contaminated aquifers.
Patent No.: US 12,421,135 B2 · Issued Sep 23, 2025
Metal Powder Mixture as Heat Source for Treating Environmental Medium
Gary M. Birk, David F. Alden, and John Sankey
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This patent describes a method for enhancing in situ thermal remediation of contaminated soil and groundwater through the use of reactive metal powder mixtures that generate additional heat through exothermic chemical reactions.
The technology combines microscale zero-valent metal particles, such as iron, with optional powdered activated carbon and chemical catalysts. When activated by an external heat source, the metal powder undergoes an exothermic oxidation reaction, generating additional heat within the treatment zone.
The approach is designed to supplement conventional thermal remediation technologies, including thermal conduction heating (TCH), electrical resistance heating (ERH), and steam-enhanced extraction (SEE). The additional heat promotes volatilization of organic contaminants, which can then be recovered through vapor extraction systems.
Potential applications include the treatment of chlorinated solvents, petroleum hydrocarbons, polycyclic aromatic hydrocarbons (PAHs), and other persistent organic contaminants.
Patent No.: US 12,103,057 B2 · Issued Oct 1, 2024
Zero-Valent Metal Suspension in Non-Aqueous Phase for Water Remediation
David F. Alden and Gary M. Birk
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This patent describes a method for preparing and applying stable suspensions of zero-valent metal particles in a non-aqueous carrier for in situ remediation of contaminated soil and groundwater.
The technology combines microscale zero-valent iron (ZVI) with vegetable oil, a thickening agent, and a surfactant to create a suspension that limits particle agglomeration, sedimentation, and premature corrosion during storage, transportation, and application.
The non-aqueous carrier also provides both readily available and slow-release electron donors to support anaerobic biodegradation. This combination promotes in situ chemical reduction (ISCR) through complementary abiotic and biological pathways for the treatment of chlorinated solvents and other contaminants.
The approach is designed to improve the handling, delivery, and subsurface distribution of reactive iron particles while maintaining their reactivity until emplacement in the treatment zone.
Patent No.: US 11,577,231 B2 · Issued Feb 14, 2023
Enhanced reduction bioremediation method using in-situ alcoholysis
Gary M. Birk and David F. Alden
View Description
This patent describes a method for enhancing in situ reductive bioremediation through alcoholysis reactions that convert vegetable oils into a combination of soluble and slow-release electron donors within contaminated soil and groundwater.
The technology combines vegetable oils, alcohols, and alkaline catalysts to promote the formation of fatty acid alkyl esters, glycerol, and carboxylic acid salts. These reaction products provide readily available and longer-lasting electron donors to support anaerobic microbial processes, including enhanced reductive dechlorination of chlorinated solvents.
The approach is designed to improve electron donor distribution within the aquifer, sustain reducing conditions, and provide buffering capacity to help maintain groundwater pH favorable for microbial activity.
The technology provides an alternative to conventional emulsified vegetable oil (EVO) applications by combining electron donor delivery with in situ chemical reactions that support contaminant biodegradation.
Patent No.: US 11,491,522 B2 · Issued Nov 8 , 2022
Zero-Valent Metal Suspension in Non-Aqueous Phase for Water Remediation
Sangho Bang, David F. Alden, Gary M. Birk, Jeffrey H. Harwell, and Bor Jier Shiau
View Description
This patent describes a composition and method for preparing stable suspensions of zero-valent metal particles in a non-aqueous carrier for in situ remediation of contaminated soil and groundwater.
The technology combines microscale zero-valent iron (ZVI), vegetable oil, propylene glycol, and a surfactant to form a suspension that minimizes particle agglomeration, sedimentation, and premature corrosion during storage, transportation, and application.
The formulation incorporates both readily available electron donors from propylene glycol and longer-lasting electron donors from vegetable oil. This combination supports in situ chemical reduction (ISCR) through complementary abiotic reactions involving ZVI and biological processes that promote contaminant degradation.
The approach is designed to improve the handling and subsurface delivery of reactive iron particles while preserving their reactivity until they reach the treatment zone. Potential applications include the remediation of chlorinated solvents and other persistent groundwater contaminants.
Patent No.: US 11,123,779 B2 · Issued Sep 21, 2021
Method and a Chemical Composition for Accelerated In Situ Biochemical Remediation
David F. Alden, Gary M. Birk, Sangho Bang, Jeffrey H. Harwell, and Bor Jier Shiau
View Description
This patent describes a method and chemical composition for accelerating in situ biochemical remediation of contaminated soil and groundwater.
The technology combines microscale zero-valent iron (ZVI), vegetable oil, propylene glycol, and a surfactant to create a stable, non-aqueous suspension. The formulation is designed to reduce particle agglomeration, sedimentation, and premature corrosion during storage, transportation, and subsurface application.
The composition provides complementary electron donors: propylene glycol offers a readily available source of electrons, while vegetable oil provides a longer-lasting source that can support sustained biological activity. Together with the reactive iron particles, these components promote in situ chemical reduction (ISCR) and biochemical degradation of contaminants.
The approach is intended to improve the handling and delivery of reactive iron particles while preserving their reactivity until they reach the treatment zone. Potential applications include the remediation of chlorinated solvents and other persistent contaminants in soil and groundwater.
Patent No.: US 9,309,136 B2 · Issued Apr 12, 2016
Bioremediation of Soil and Groundwater
John Archibald and Gary M. Birk
View Description
This patent describes a composition and method for preparing self-emulsifying vegetable oil formulations used in the enhanced in situ bioremediation of contaminated soil and groundwater.
The technology combines vegetable oil with a specialized blend of nonionic surfactants and co-surfactants to produce a concentrated formulation that spontaneously forms a fine oil-in-water emulsion when mixed with water under gentle agitation.
The resulting emulsion is designed to improve the distribution of vegetable oil electron donors within contaminated aquifers, providing a sustained carbon source to support anaerobic microbial activity and enhanced reductive dechlorination of chlorinated solvents.
The approach simplifies field preparation of emulsified vegetable oil (EVO) amendments by eliminating the need for specialized high-shear mixing equipment. The formulation is intended to improve electron donor delivery and distribution while supporting long-term biological treatment of groundwater contaminants.
Patent No.: US 7,708,496 B2 · Issued May 4, 2010
In-Situ Surfactant and Chemical Oxidant Flushing for Complete Remediation of Contaminants and Methods of Using Same
Bor-Jier Shiau
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This patent describes an integrated method for remediating contaminated soil and groundwater through the sequential application of biodegradable co-solvents, surfactant solutions, and chemical oxidants.
The technology begins with the introduction of a biodegradable co-solvent, followed by a surfactant solution selected to improve contaminant solubilization and mobilization. A chemical oxidant is subsequently introduced to degrade residual contaminants remaining after the flushing process.
The method incorporates site-specific evaluations of surfactant performance, including contaminant solubilization, surfactant sorption and precipitation, non-aqueous phase liquid (NAPL) behavior, and contaminant extraction under simulated aquifer flow conditions. Chemical oxidant selection considers reaction kinetics, oxidant persistence, pH requirements, and groundwater geochemistry.
The approach is particularly applicable to complex, viscous, or poorly soluble organic contaminants, including petroleum hydrocarbons and coal tar residues, where conventional surfactant flushing alone may be insufficient to achieve remediation objectives.
Patent No.: US 7,677,836 B2, · Issued Mar 2010
In-Situ Surfactant and Chemical Oxidant Flushing for Complete Remediation of Contaminants and Methods of Using Same
Bor-Jier Shiau
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This patent describes a method for enhancing in situ remediation of contaminated soil and groundwater through the combined application of a specialized surfactant formulation and biodegradable co-solvents.
The technology uses a surfactant mixture containing sodium dioctyl sulfosuccinate and linear alkyl diphenyloxide disulfonate to improve the solubilization and removal of hydrophobic organic contaminants from subsurface formations.
A biodegradable co-solvent is introduced into the treatment zone to supplement the surfactant flushing process. The combined treatment is designed to improve the removal of non-aqueous phase liquids (NAPLs), including contaminants with low aqueous solubility or elevated viscosity.
The method also provides for an optional chemical oxidation treatment to degrade residual contaminants following surfactant and co-solvent application. Potential oxidants include hydrogen peroxide and potassium permanganate.
The technology supports an integrated remediation approach combining contaminant mobilization, enhanced extraction, and chemical treatment to reduce residual contaminant concentrations.
Patent No. : US 7,364,386 B2 · Issued Apr 29, 2008
In-Situ Surfactant and Chemical Oxidant Flushing for Complete Remediation of Contaminants and Methods of Using Same
Bor-Jier Shiau
View Description
This patent describes a method for remediating contaminated soil and groundwater through the application of a specialized aqueous surfactant formulation designed to enhance the removal of non-aqueous phase liquids (NAPLs).
The technology uses a mixture of sodium dioctyl sulfosuccinate and linear alkyl diphenyloxide disulfonate in water to improve the solubilization and mobilization of hydrophobic organic contaminants within subsurface formations.
The claimed method specifies surfactant concentrations ranging from approximately 0.05% to 15% by weight, including narrower concentration ranges suited to different treatment conditions. The formulation is intended for the removal of both dense non-aqueous phase liquids (DNAPLs), such as chlorinated solvents, and light non-aqueous phase liquids (LNAPLs), including petroleum hydrocarbons.
The approach provides a means of enhancing contaminant recovery through surfactant flushing, reducing residual contaminant mass and supporting subsequent remediation activities where needed.
Patent No.: US 7,021,863 B2 · Issued Apr 4, 2006
In-Situ Surfactant and Chemical Oxidant Flushing for Complete Remediation of Contaminants and Methods of Using Same
Bor-Jier Shiau
View Description
This patent describes a method for enhancing in situ remediation of contaminated soil and groundwater through the use of a selected surfactant mixture that improves the solubilization and removal of organic contaminants.
The technology combines sodium dioctyl sulfosuccinate and linear alkyl diphenyloxide disulfonate to create a surfactant solution capable of increasing the apparent aqueous solubility of hydrophobic contaminants and facilitating their removal from contaminated subsurface formations.
The method is applicable to both dense non-aqueous phase liquids (DNAPLs), including chlorinated solvents, and light non-aqueous phase liquids (LNAPLs), such as petroleum hydrocarbons. The patent describes surfactant concentrations ranging from approximately 0.05% to 15% by weight.
By enhancing contaminant solubilization and recovery, the approach is intended to reduce the mass of persistent organic contaminants in soil and groundwater and improve the effectiveness of surfactant-enhanced aquifer remediation (SEAR).
Patent No.: US 6,913,419 B2 · Issued Jul 5, 2005
In-Situ Surfactant and Chemical Oxidant Flushing for Complete Remediation of Contaminants and Methods of Using Same
Bor-Jier Shiau
View Description
This patent describes an integrated method for remediating contaminated soil and groundwater through the combined application of surfactant-enhanced aquifer remediation (SEAR) and in situ chemical oxidation (ISCO).
The technology uses selected surfactant formulations to improve the solubilization and removal of hydrophobic organic contaminants, including dense and light non-aqueous phase liquids (DNAPLs and LNAPLs). Chemical oxidants are then used to degrade residual contaminants that may remain following surfactant flushing.
The patent includes specific surfactant combinations, including sodium dioctyl sulfosuccinate with linear alkyl diphenyloxide disulfonate, as well as alkylamine sodium sulfonate with sodium dihexyl sulfosuccinate. Potential chemical oxidants include hydrogen peroxide and potassium permanganate.
The method incorporates site-specific evaluation of surfactant performance, contaminant recovery, oxidant reaction kinetics, and groundwater geochemistry to support the selection of appropriate treatment formulations.
The approach combines contaminant mass removal with chemical destruction of residual contamination to address limitations associated with surfactant flushing alone.
Tersus Trademarks
Tersus Environmental’s trademarks identify proprietary technologies, products, and services developed to support the in situ remediation of soil and groundwater contamination. These marks help distinguish Tersus Environmental’s offerings and reflect our commitment to quality, technical expertise, and consistent performance.
The following is a non-exhaustive list of trademarks owned by Tersus Environmental. When using these marks in publications distributed within the United States, include the appropriate ™ or ® symbol on first use. For publications distributed outside the United States, do not include trademark symbols; instead, use an appropriate trademark attribution notice (for example: Nutrimens and NutriSulfate are trademarks of Tersus Environmental, LLC, registered in the United States and other countries).
The absence of a product or service name or logo from this list does not constitute a waiver of Tersus Environmental’s trademark or other intellectual property rights associated with that name or logo.
Registered U.S. Trademarks
- NutriBind® (Serial No. 86904938)
- Nutrimens® (Serial No. 86033363)
- Nutrisulfate® (Serial No. 86033330)
Other Trademarks
- EDS-Activator™
- EDS-Advanced™
- EDS-ER™
- EDS-ME™
- EDS-QR™
- EDS-ZVI™
- MicroEVO™
- NanoEVO™
- TASK™
- TersOx™
